Chemical constituents from leaves of Lindera aggregate / 中草药

Objective To study the chemical constituents in the leaves of Lindera aggregate.MethodsVarious column chromatographic techniques were used to separate and purify the chemical constituents and their structures were elucidated by spectral analyses.Results Nine compounds were isolated and identified as quercetin(Ⅰ),and kaempferol(Ⅱ),avicularin(Ⅲ),afzelin(Ⅳ),dihydrokaempferol(Ⅴ),astragaline(Ⅵ),kaempferol-3-O-?-D-xylopyranoside(Ⅶ),juglalin(Ⅷ),and kaempferol-3-O-(2″-O-?-D-glucopyranosyl)-?-L-rhamnopyranoside(Ⅸ).Conclusion Compounds Ⅲ—ⅠⅩ are isolated from the title plant for the first time.Compounds Ⅴ—Ⅸ are isolated from the plants of Lindera Thunb.for the first time.

Study on Quality Control of Qilian Suppository / 中国药房

OBJECTIVE:To establish the method to control the quality of Qilian suppository.METHODS:TLC was per?formed to identify Rhizoma coptidis and Radix Notoginseng.A reverse phase HPLC-ELSD method was adopted to determine the content of ginsenoside Rg 1 and ginsenoside Rb 1 in Radix Notoginseng.RESULTS:The study on the quality control showed that the characteristic of identification by TLC was distinct and highly specific.In this quantification method,the linear ranges of ginsenoside Rg 1 and Rb 1 were1.56?g～3.74?g(r=0.9993,RSD=1.6%)and1.44?g～3.46?g(r=0.9981,RSD=1.2%)respectively.The average recovery rate of ginsenoside Rg 1 was99.10%,and RSD=1.6%(n=3);the average recovery rate of ginsenoside Rb 1 was102.13%,and RSD=1.2%(n=3).CONCLUSION:The method is simple,sensitive,accurate and re?peatable.It can be used for the quality control of Qilian suppository.